Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. Based on your materials, application, and requirements, the other 4 methods provide specific focuses.

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Please share this page: Table 1 below shows the various methods for four common standards: The etch structure types used to classify the specimens are: There are a number of recognised tests when it comes to the intergranular corrosion testing of corrosion resistant alloys CRA.

It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation 2a62 chromium carbides at grain boundaries. Methods for ast, the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. By using our website you consent to all cookies in accordance with our Cookie Policy.

ASTM G28 does not require samples to be heat treated. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of axtm such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.

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Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five wstm boiling intervals. As 15 hours is a difficult test period in practice, and is only a minimum, conducting the sstm for 20 hours overnight means that the two tests are equivalent. See Appendix X1 for information regarding test selection. All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior.


We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments. The level of corrosion is determined by mass loss. This website uses cookies to improve user experience.

Intergranular Attack – ASTM A – Colorado-Metallurgical-Services

Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:.

Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: These tests were introduced when the carbon content in CRAs typically hit 0. Wilson Hardness Conversion Chart. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.

It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. For alloys not listed in this standard, it will be necessary to carry out some tests on material in various conditions to determine the threshold. The effect of post weld surface treatments on the corrosion resistance of super duplex stainless steel welds in sea water The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult.

ASTM A Intergranular Corrosion Testing and Analysis

Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.

The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. ASTM G28 method B is a more aggressive test than method A and is intended for more corrosion aztm alloys, as listed in the document.


This method is preferable for chromium depletions and corrosion in intermetallic phases. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly asstm materials; ASTM A is a screening test to help find batches that are incorrectly processed. There is several cause for SCC, Chloride is the leading cause of transgranular cracking or attack.

Zstm tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking. This document describes all three of these tests for four common standards, and describes the differences.

For many alloys, the onset is at 0. Conducting the Tests When a test has been selected, follow the detailed directions in that standard for making up the test solution, the astj of test samples and the finish to a62 used. ASTM G28 was designed for nickel-based alloys, and a list of applicable alloys for methods A and B is in the standard.

The most convenient size is often a cylinder 10mm diameter by mm long, but other dimensions are possible to suit particular product forms. Discover perspectives, resources, and advice from our world-leading Engaged Experts. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.

The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. Why were these tests designed?

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments ast as nitric acid. It depends on which Practice is selected, but typically ranges from to days for different tests.